| 动物源性食品中尼卡巴嗪残留量的测定 |
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| 引用本文： | 魏博娟,钱卓真,吴成业.动物源性食品中尼卡巴嗪残留量的测定[J].福建水产,2009(4):72-75. |
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| 作者姓名： | 魏博娟 钱卓真 吴成业 |
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| 作者单位： | 1. 集美大学,福建,厦门,361021;福建省水产研究所,福建,厦门,361012
2. 福建省水产研究所,福建,厦门,361012 |
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| 摘 要： | 动物产品中的尼卡巴嗪药物残留已被我国及美国、日本、欧盟等国家和地区列为重点检测内容，其最大残留量为0．01mg／kg-0．2mg／kg不等。为探讨合适的检测方法，本文对国内外相关尼卡巴嗪的分析检测方法的优缺点做了分析和比较，并重点介绍了动物源性食品中尼卡巴嗪残留量检测的高效液相色谱法（HPLC）和高效液相色谱-质谱联用（HPLC-MS）法。运用这两种方法进行检测，其最低检测限可达到10μg／kg甚至0．5μg／kg，基本上符合现有相关标准的限量要求。
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| 关 键 词： | 尼卡巴嗪 药物残留 动物产品 检测方法 |
Determination of Residual Nicarbazin in Animal-derived Food |
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| WEI Bo-juan,QIAN Zhuo-zhen,WU Cheng-ye.Determination of Residual Nicarbazin in Animal-derived Food[J].Journal of Fujian Fisheries,2009(4):72-75. |
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| Authors: | WEI Bo-juan QIAN Zhuo-zhen WU Cheng-ye |
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| Institution: | WEI Bo-juan , QIAN Zhuo-zhen, WU Cheng-ye ( 1. Jimei University, Xiamen 361021, China; 2. Fisheries Research Institute of Fujian, Xiamen 361012, China) |
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| Abstract: | Residual Nicarbazin in animal-derived food has been listed as the major monitoring content by our country, America, Japan, European Union and so on . The maximum residual limit （MAL） is ranged from 0. 01mg/kg to 0. 2mg/kg. In order to investigate the suitable test method, this essay analyzed and compared the merit and demerit of the different detection methods that had been reported from home and abroad. It puts the emphasis on the use of a high - performance liquid chromatography （HPLC） and liquid chromatography tandem mass spectrometry （HPLC-MS）. With the two ways above, the lowest detection limit can reach 10μg/kg even 0. 5μg/kg , which can meet the demands of the related basic standards. |
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| Keywords: | Nicarbazin Drug residual Animal - derived food Detection methods |
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