气相色谱法测定蔬菜中有机磷的研究 |
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引用本文: | 姚新建,张保东,詹秀环,霍俊杰.气相色谱法测定蔬菜中有机磷的研究[J].安徽农业科学,2008,36(36). |
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作者姓名: | 姚新建 张保东 詹秀环 霍俊杰 |
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作者单位: | 周口师范学院化学系,河南周口,466000;周口师范学院化学系,河南周口,466000;周口师范学院化学系,河南周口,466000;周口师范学院化学系,河南周口,466000 |
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摘 要: | 目的]建立检测蔬菜中有机磷的气相色谱方法。方法]采用气相色谱-火焰光度检测器检验蔬菜中的有机磷。结果]结果表明,农药的加标回收率为73.88%~108.90%,相对标准偏差为2.07%~5.08%,检出限为0.017 3~0.039 5μg/ml。结论]该方法操作简便、快速,方法回收率和精密度较好。
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关 键 词: | 气相色谱 有机磷农药 残留 |
Determination on the Organic Phosphorus in Vegetables with Gas Chromatography |
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Abstract: | Objective] The purpose aimed to establish a simple gas chromatography method for determining organic phosphorus in vegetables.Method] The gas chromatography-flame photometric detector was used to determine organic phosphorus in vegetables.Result]The results indicated that the recovery of standard addition,relative standard deviation and detection limit of this method were 73.88%-108.90%,2.07%-5.08% and 0.017 3-0.039 5 μg/ml,respectively.Conclusion]The operation of this method is simple and rapid,the recovery and precision is better. |
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Keywords: | Gas chromatography Organophosphorus pesticide Residues |
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