| 香味剂中大茴香脑、d-柠檬烯、香芹酚含量测定的研究 |
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| 引用本文： | 信 佳 张新竹 富 岩,等.香味剂中大茴香脑、d-柠檬烯、香芹酚含量测定的研究[J].现代畜牧兽医,2014(3):9-11. |
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| 作者姓名： | 信 佳 张新竹 富 岩 等 |
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| 作者单位： | [1] 辽宁省抚顺市畜产品质量安全检测中心,辽宁 抚顺113006 [2] 辽宁省鞍山市畜产品有害物质检测中心,辽宁 鞍山114000 |
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| 摘 要： | 本研究建立了气相色谱法测定饲料香味剂中大茴香脑、d-柠檬烯、香芹酚的方法。试样经丙酮提取后，用GC测定大茴香脑、d-柠檬烯和香芹酚。大茴香脑、d-柠檬烯和香芹酚的线性范围为1.0～500.0μg/mL。大茴香脑、d-柠檬烯和香芹酚在浓度为1～10 g/kg添加水平时的回收率分别在96.2%～101.5%、97.1%～102.5%和96.5%～99.8%，RSD分别为1.3%、1.5%和1.1%。方法定量限为50 mg/kg。本方法对饲料香味剂中大茴香脑、d-柠檬烯和香芹酚的检测分析准确性高、重现性好。
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| 关 键 词： | 大茴香脑 d-柠檬烯 香芹酚 |
Determination of Anethole,D-limonene and Carvacrol in Fodder Flavouring Agent |
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| Institution: | Xin Xia, Zhang Xinzhu, Fu Yan, Jin Chuan, Wang Hongyan, Fang Sujiao (1. Detecting Center of the quality and safety of animal products in Fushun City, Liaoning Fushun 113006; 2. Testing center of the livestock hazardous substances in Anshan City, Liaoning Anshan 114000) |
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| Abstract: | An effective method was developed to determine anethole、d-limonene and carvacrol in fodder flavouring agent by GC. The anethole、d-limonene and carvacrol were extracted from fodder flavouring agent with acetone and were determined by GC. Recoveries of anethole、d-limonene and car-vacrol were 96.2%~101.5%, 97.1%~102.5% and 96.5%~99.8%.Relative standard deviations were 1.3%, 1.5% and 1.1%. The lower determination limits were 50mg/kg. The method is effective and accurate for determining anethole, d-limonene and carvacrol in fodder flavouring agent. |
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| Keywords: | Anethole D-limonene Carvacrol |
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