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澳洲坚果油超声波辅助提取工艺优化及其理化性质
引用本文:涂行浩,孙丽群,唐景华,张明,帅希祥,陈洪,杜丽清.澳洲坚果油超声波辅助提取工艺优化及其理化性质[J].热带作物学报,2019,40(11):2217-2226.
作者姓名:涂行浩  孙丽群  唐景华  张明  帅希祥  陈洪  杜丽清
作者单位:1. 中国热带农业科学院南亚热带作物研究所/农业农村部热带果树生物学重点实验室,广东湛江 5240912. 中国农业科学院油料作物研究所/油料脂质化学与营养湖北省重点实验室,湖北武汉 4300623. 云南农业大学热带作物学院,云南普洱 665000
基金项目:油料脂质化学与营养湖北省重点实验室开放基金资助(201702);中央级公益性科研院所基本业务费(1630062017009);中央级公益性科研院所基本业务费(1630062019029)
摘    要:为提高澳洲坚果油提取得率并获得高品质油脂,采用超声波辅助法提取澳洲坚果油,并分析提取油脂的理化性质。首先通过单因素实验考察了提取溶剂、超声功率、超声时间以及液料比对提取率的影响,然后通过响应面法优化了提取工艺参数。结果表明,正己烷对澳洲坚果油提取率较高;适当增加超声波功率、超声时间以及溶剂量,澳洲坚果油得率均随之增加;通过响应面优化,超声波辅助提取澳洲坚果油的最佳提取条件为:液料比为9.6∶1(mL/g),超声功率为520 W,超声时间为32 min,澳洲坚果油得率达69.1%,2次提取总得率达96.3%。研究结果表明超声波辅助提取是一种有效的油脂提取方法,从脂肪酸成分比例及理化性质来看,澳洲坚果油营养价值较高。

关 键 词:澳洲坚果油  超声辅助提取  响应面优化  理化性质  
收稿时间:2019-02-18

Optimization of Ultrasonic Assisted Extraction of Macadamia Oil and Its Physicochemical Properties
TU Xinghao,SUN Liqun,TANG Jinghua,ZHANG Ming,SHUAI Xixiang,CHEN Hong,DU Liqing.Optimization of Ultrasonic Assisted Extraction of Macadamia Oil and Its Physicochemical Properties[J].Chinese Journal of Tropical Crops,2019,40(11):2217-2226.
Authors:TU Xinghao  SUN Liqun  TANG Jinghua  ZHANG Ming  SHUAI Xixiang  CHEN Hong  DU Liqing
Institution:1. South Subtropical Crops Research Institute, Chinese Academy of Tropical Agricultural Sciences / Key Laboratory of Tropical Fruit Biology, Ministry of Agriculture and Rural Affairs, Zhanjiang, Guangdong 524091, China2. Oil Crops Research Institute, Chinese Academy of Agricultural Sciences / Hubei Key Laboratory of Lipid Chemistry and Nutrition, Wuhan, Hubei 430062, China3. Tropical Crop College, Yunnan Agricultural University, Puer, Yunnan 665000, China
Abstract:In order to improve the extraction rate of macadamia oil and obtain high quality oil, an ultrasonic assisted method was used to extract macadamia oil, and the physicochemical properties of the extracted oil were analyzed. The effects of extraction solvent, ultrasonic power, ultrasonic time and ratio of liquid to material on the extraction rate were investigated by single factor experiments, and then the extraction process parameters were optimized by response surface methodology (RSM). The results showed that the extraction rate of macadamia oil was higher with n-hexane, and the yield of macadamia oil increased with the proper increase of ultrasonic power, ultrasonic time and solvent content. The optimum extraction conditions of macadamia oil were as follows: the ratio of liquid to material 9.6∶1 (mL/g), the ultrasonic power 520 W, the ultrasonic time 32 min, and the yield of macadamia oil was 69.1% under the conditons. The total yield extracted twice reached 96.3%. The results showed that ultrasonic assisted extraction was an effective method for macadamia oil extraction. In terms of fatty acid composition and physicochemical properties, macadamia oil is a kind of natural vegetable oil with high nutritional value.
Keywords:macadamia (Macadamia integrifolia) oil  ultrasound-assisted extraction  response surface optimization  physicochemical properties  
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