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当归藤不同部位挥发油成分GC-MS分析
引用本文:卢森华,李耀华,陈勇,曾海生,张龙,郑锡任.当归藤不同部位挥发油成分GC-MS分析[J].安徽农业科学,2012,40(2):733-735.
作者姓名:卢森华  李耀华  陈勇  曾海生  张龙  郑锡任
作者单位:广西中医学院药学院,广西南宁,530001;广西中医学院药学院,广西南宁,530001;广西中医学院药学院,广西南宁,530001;广西中医学院药学院,广西南宁,530001;广西中医学院药学院,广西南宁,530001;广西中医学院药学院,广西南宁,530001
基金项目:广西自然科学基金创新研究团队项目,广西中医药管理局2011年度中医药自筹经费科研课题
摘    要:目的]研究当归藤不同部位中挥发油成分。方法]采用水蒸气蒸馏法分别提取当归藤根、茎、叶的挥发油成分,通过气相色谱-质谱联用法对这3个部位挥发油的化学成分进行对比研究,并用面积归一化法获得各化合物的相对含量。结果]从当归藤根中鉴定出11个成分,占挥发油总量的77.67%;从当归藤茎中鉴定出36个成分,占挥发油总量的92.88%;从当归藤叶中鉴定出74个成分,占挥发油总量的85.11%。结论]该方法结果准确可靠,为当归藤的质量标准制定及进一步开发利用提供了科学依据。

关 键 词:当归藤(Embelia  parviflora  Wall.  ex  A.DC.)  挥发油  GC-MS

Study on the Chemical Constituents of Volatile Oil from Different Parts of Embelia parviflora Wall.ex A.DC.by GC-MS
Institution:LU Sen-hua et al(Faculty of Pharmacy,Guangxi Traditional Chinese Medicine University,Nanning,Guangxi 530001)
Abstract:Objective] To study the chemical constituents of volatile oil from different parts of Embelia parviflora Wall.ex A.DC.Method] The volatile oil was respectively extracted from the root,stem and leaf of E.parviflora by steam distillation and then analyzed by gas chromatography-mass spectrometry(GC-MS).The relative content of all isolated compounds was determined by area normalization.Result] 11 chemical constituents were identified from the root of E.parviflora,accounting for 77.67% of total volatile oil.36 chemical constituents were identified from the stem,accounting for 92.88%of total volatile oil.74 chemical constituents were identified from the leaves,accounting for 85.11% of total volatile oil.Conclusion] The study result was accurate and reliable,which could provide scientific basis for the establishment of quality standard,further development and utilization of E.parviflora.
Keywords:Embelia parviflora Wall  ex A  DC    Volatile oil  GC-MS
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