| 液相色谱-串联质谱法测定畜禽肉中十种磺胺类兽药残留的不确定度评定 |
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| 引用本文： | 任雪冬.液相色谱-串联质谱法测定畜禽肉中十种磺胺类兽药残留的不确定度评定[J].中国兽药杂志,2011,45(5):20-25. |
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| 作者姓名： | 任雪冬 |
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| 作者单位： | 辽宁省分析科学研究院,沈阳,110015 |
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| 摘 要： | 依据GB/T20759-2006方法对畜禽肉中十种磺胺类兽药残留检测的不确定度进行了分析和评定。结果表明标准品的配制、稀释,标准曲线校准,样品回收率对样品的相对不确定度贡献较大。
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| 关 键 词： | 磺胺类兽药残留 液相色谱-串联质谱法 不确定度评定 |
| 收稿时间： | 2010/10/14 0:00:00 |
| 修稿时间： | 3/8/2011 12:00:00 AM |
Uncertainty Evaluation in the Determination of Ten Kinds of Sulfanilamide Residues in Poultry by Liquid Chromatography-Tandem Mass Spectrometry |
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| renxuedong.Uncertainty Evaluation in the Determination of Ten Kinds of Sulfanilamide Residues in Poultry by Liquid Chromatography-Tandem Mass Spectrometry[J].Chinese Journal of Veterinary Drug,2011,45(5):20-25. |
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| Authors: | renxuedong |
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| Institution: | Liao Ning Province Academy of Analytic Science |
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| Abstract: | The article analyses and evaluates uncertainty in the determination of ten kinds of sulfanilamides residues in poultry according to the method of GB/T20759-2006.The result makes known that the contribution is major about the preparation of solutions,calibration of standard curves,and coefficients of recoveries in spiked samples. |
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| Keywords: | sulfanilamides residues Liquid Chromatography-Tandem Mass Spectrometry uncertainty evaluation |
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