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1.
提出了以聚乙烯吡咯烷酮(PVPr)修饰碳糊电极测定水中苯酚的方法.在0.1mol/LKCl的酚试液中开路富集后,在磷酸盐缓冲液介质(pH5.6)中溶出,用微分脉冲伏安法测定,苯酚的溶出峰电位为+0.73V(Ag-AgCl参比电极),检测限为0.05μg/L.应用该法测定了废水中苯酚的含量,并讨论了该法测定苯酚的影响因素,比较了几种修饰电极测定苯酚的灵敏度,探讨了苯酚在该修饰电极上的富集机理 相似文献
2.
本文用离子选择电极法测定了N,N—二甲基膦酸基甘氨酸(NBPG)与银、镉、汞的配合物组成和稳定常数。结果表明,NBPG与Ag~ 、Cd~(2 )、Hg~(2 )均生成组成为1:1的多齿质子型配合物。其lgK_稳值分别为:AgL5.28、CdH_3L3.63、CdH_2L5.16、CdHL7.30、CdL11.56、HgH_3L6.06、HgH_2L7.55、HgHL8.24、HgL12.58。 相似文献
3.
The effects of electrode configuration and click polarity on brainstem auditory evoked potentials (BAEP) in dogs were investigated to clarify the inconsistent nomenclature for each peak. Four positive peaks (waves 1, 2, 3 and 4) before a deep negative trough and a fifth positive peak (wave 5) following the trough were the basic components of BAEP in dogs, which were easily identified regardless of recording conditions such as electrode configuration and click polarity. Additional peaks tended to be present when a noncephalic reference electrode and/or single-polarity (rarefaction or condensation) click stimuli were used. The Roman nomenclature for the individual positive peaks of BAEP in dogs is confused owing to variations in the observed waveforms among researchers, but click polarity and/or reference electrode position can explain all the previously reported variations in BAEP waveforms in dogs. When the criteria concerning wave V in the guidelines of BAEP in human beings are applied to avoid further confusion of Roman nomenclature in dogs, it is recommended that the basic five positive peaks (waves 1, 2, 3, 4 and 5 as identified easily with Ai-Vertex configuration and alternating clicks) are designated as waves I, II, III, V and VI, respectively. Wave IV (wave 3b) occurs occasionally before wave V in dogs.Abbreviations BAEP
brainstem auditory evoked potentials
- dBHL
dB hearing level
- IPL
interpeak latency
- Ai
the caudodorsal end of the zygomatic arch ipsilateral to the stimulated ear
- Nape
the neck over the spinous process of the fourth cervical vertebra 相似文献
4.
The salt‐sensitive Glycine max N23674 cultivar, the salt‐born Glycine soja BB52 population, and their hybrid 4076 strain (F5) selected for salt tolerance generation by generation were used as the experimental materials in this study. First, the effects of NaCl stress on seed germination, tissue damage, and time‐course ionic absorption and transportation were compared. When qualitatively compared with seed germination appearance in culture dishes, and tissue damages on roots or leaves of seedlings, or quantitatively compared with the relative salt injury rate, the inhibition on N23674 was all the most remarkable. After the exposure of 140 mm NaCl for 1 h, 4 h, 8 h, 12 h, 2 days and 4 days, the content of Cl? gradually increased in the roots and leaves of seedlings of BB52, 4076 and 23674. Interestingly, the extents of the Cl? rise in roots of the three experimental soybean materials were BB52 > 4076 > N23674, whereas those in leaves were just on the contrary. Secondly, by using the scanning ion‐selective electrode technique (SIET), fluxes of Na+ and Cl? in roots and protoplasts isolated from roots and leaves were also investigated among the three experimental soybean materials. After 140 mm NaCl stress for 2, 4 and 6 days, and when compared with N23674, slighter net Cl? influxes were observed in root tissue and protoplasts of roots and leaves of BB52 and 4076 seedlings, especially at the cellular protoplast level. The results indicate that with regard to the ionic effect of NaCl stress, Cl? was the main determinant salt ion for salt tolerance in G. soja, G. max and their hybrid, and the difference in their Cl?/salt tolerance is mainly attributed to the capacity of Cl? restriction to the plant above‐ground parts such as leaves. 相似文献
5.
《Communications in Soil Science and Plant Analysis》2012,43(6):415-420
Abstract The usefulness of the nitrate‐specific ion electrode (NE) for the determination of nitrate nitrogen (NO3‐N) in surface and ground water was determined. The NE method had several advantages that made it superior to the phenoldisulfonic acid (PDS) method in our environmental quality studies. Samples could be analyzed quickly and with a minimum of sample preparation. Sample coloration and soluble salts did not interfere with the performance of the electrode. Range of detection without dilution was much wider than by the PDS method. Also, the values obtained by the NE method, although slightly greater than those obtained by the PDS method, were satisfactory. 相似文献
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冶金因素对纯镍铸铁焊条抗热裂性能影响 总被引:1,自引:0,他引:1
研究了钛、铌,钛,钼,硅和钇镁硅铁合金对纯镍铸铁焊条抗热裂性能的影响,试验结果表明,钛,铌,钴,钇和镁在焊缝中的含量有一最佳值,综合利用这些合金元素,可显著改善纯镍铸铁焊条的抗热裂性能,其熔敷金属的机械性能可符合铁素体球墨铸铁(QT400-15)的要求。 相似文献
9.
《Communications in Soil Science and Plant Analysis》2012,43(5):477-481
Abstract An ammonia electrode was evaluated as a means of determining ammonium concentration in semi‐micro Kjeldahl digests of plant samples. Results of the ammonia electrode determination agreed closely with distillation and titration results. Advantages of the electrode method include speed, precision, increased safety, simplicity and the fact that only a small aliquot of the digest is used. 相似文献
10.
《Communications in Soil Science and Plant Analysis》2012,43(6):569-578
Abstract Work to evaluate the Orion nitrogen oxide electrode indicated that this electrode can be used satisfactorily for determination of nitrite in soil extracts and water samples. The electrode method of analysis described is simple, rapid, and precise, and its results agree closely with those obtained by the colorimetric method of Griess‐Ilosvay. The electrode method has the advantage that its results are not affected by color or turbidity or by Cu2+ and Hg2+ present in samples under analysis 相似文献