毛细管气相色谱内标法测定防霉剂中富马酸二甲酯

建立了巴豆酸为内标物,用毛细管气相色谱快速测定防霉剂中富马酸二甲酯含量的方法.样品用乙酸乙酯提取,以DM-FFAP毛细管柱分离,火焰离子化检测器检测.结果表明,在0.25～3.0 mg/mL浓度范围内,富马酸二甲酯和巴豆酸的浓度比与峰面积比的回归方程为y=-0.0009 0.7174x,相关系数r=0.9996,检出限为5.0 mg/L;样品加标回收率(n=6)为97.0%～104.0%,相对标准偏差为3.26%.该方法简单、快速、准确度好,可用于测定防霉剂中的富马酸二甲酯含量.     

PAYING ATTENTION TO USE SIMPLEX METHOD FOR OPTIMAL MULTIPARAMETER IN THE DESIGN OF CONTROL SYSTEM

In the design of control system using simplex method for optimal multi-parameter,if the difference in number between the greatest and the smallestparameters is very great,the optimization process converges very slowly.Evenoptimal parameters can't be found at all.This paper studies the problem,analyses its cause and poses a resolution means.A testing example shows thatthis means can solve the above problem well.     

SOME PROBLEMS BY USE OF BOUNDARY POINT ELEMENT IN BOUNDARY ELEMENT METHOD

Using boundary point element is one of the treatmentsof corner node problem.This paper further discusses some problems byuse of point element.They mainly include the calculation of stresses atpoint elements,the cause and treatment of singularity in boundary usingequations when point elements are used.An example is given.Correctlyboundary point element has certain practical significance for moreobjective simulation of the actual situation of quantities and improvesaccuracy of results.     

Research on PDM Technology Oriented Dynamical Data

对冬枣采后主要病害种类、症状及防治方法进行阐述,并介绍了生物防治技术在果蔬贮运病害防治中的应用,展望了该技术在冬枣采后病害防治中的应用前景.     

凤仙花种子的贮藏特性研究

通过比较普通开放式贮藏、0~4℃冷冻贮藏和硅胶干燥贮藏条件下的凤仙花种子的活力和细胞膜完整性的变化,发现硅胶干燥贮藏能保持凤仙花种子较高的活力和细胞膜结构的完整性,是一种理想的贮藏方法。     

Analysis of Unbalanced Data by Mixed Linear Models Using the mixed Procedure of the SAS System

Unbalanced data are a common problem in plant research based on designed experiments. Such data are often conveniently analysed using linear mixed models. Recent developments in mixed model theory have been implemented in major packages. This paper describes the use of the mixed procedure of the SAS System for the analysis of designed experiments. Special emphasis is given to the specification of options as depending on the assumed mixed model and on the unbalancedness in the data. In addition, we consider a compact representation of multiple comparisons for unbalanced data (letter display). Two small data sets are used to exemplify the methods.     

烟草含钾量反射仪-钾离子试纸法快速测定研究初报

比较了反射仪—K 试纸法(K ts-fl)、原子吸收光谱法、ICP-aeS法测定烟株叶脉汁液中的K 含量的三种方法,确定反射仪—K 试纸法测定烟株钾含量的可行性及其最佳测定范围;在烤烟不同生育期,应用反射仪—K 试纸法对烟株叶片不同部位含K 水平的测定,确定其最佳测定时期及部位。研究结果表明,反射仪—K 试纸法与原子吸收光谱法、ICP-aeS法测定结果差异不显著,应用反射仪—K 试纸法进行烟株钾素快速诊断可行,且具有时间短,简单快速,易操作等优点。反射仪测定K 的稳定线性范围是0.30～0.9g/L;在不同时期对烟株不同部位测定研究表明,最佳诊断部位为烟株第二平展叶叶脉基部2cm段。     

Yield potential and drought tolerance of segregating populations of barley in contrasting environments

Summary Using the traditional approach (selection for grain yield) it has been found that F₃ families derived from F₂'s selected under unfavourable conditions were more vigorous in the early stages of growth, taller, earlier in heading and with larger yields than F₃ families derived from F₂'s selected under favourable conditions. A high and negative correlation coefficient was found between the drought susceptibility index and grain yield at the driest site, whereas at the wettest site the correlation coefficients were lower and in some cases positive, indicating the existence of traits which are desirable under drought and undesirable under favourable conditions, or vice versa.Expected responses to selection for grain yield using different selection criteria indicated that selection under stress conditions is expected to be more efficient than selection under favourable conditions when dry areas is the target environment.Expected responses to selection for grain yield using different selection criteria indicated that selection under stress conditions is expected to be more efficient than selection under favourable conditions when dry areas is the target environment.Part of this work was supported by Opec Fund for International Development.     

A definition of the optimal allocation of effort in conservation of plant genetic resources-with application to sample size determination for field collection

Summary A criterion was presented to define the most efficient strategy for the exploration and maintenance of plant genetic resources. All of the three factors composing the efficiency. i.e., multiplicity of target populations. the amount of expenses, and goodness for individual populations of the conservation manipulation adopted, were incorporated in the present criterion. Sample size per target population for field collection was investigated on the basis of this criterion, leading to the conclusion that the number of visited populations rather than sample size per population determines the overall efficiency of a collection project as a whole. Without any particular reason, intensive sampling for a limited number of populations is not logical. A sample size as small as ten plants per site or population was estimated reasonable to cover a large target area.     

粮仓温度场数学模型研究

粮仓温度的传统测试方法存在硬件结构复杂、电气元件过多,可靠性低等缺点。本文根据测量得到的有限个典型的离散温度数据,利用最小二乘法拟合出粮仓温度在其空间坐标上的分布函数,从而可以较精确地估计粮仓内任一点的温度值,大大节约了硬件资源,方便了测量工作。