三羟鹅膏毒肽的反相高效液相色谱分离纯化

用反相高效液相色谱法,以0.02mol醋酸铵-乙腈为流动相和梯度洗脱模式,从灰花纹鹅膏菌中分离纯化出三羟鹅膏毒肽(amanin),产品纯度达96%以上,三羟鹅膏毒肽的分子量为903.3.     

Power spectrum density and experimental modal analysis of wide belt sander applied in domestic wood industry

This paper took the upper-lower wide belt sander B229 with four-feet wide belts, manufactured in China, as the study target. By means of framework dynamic design, we study its vibration characteristics by commencing from the place having horizontal defects and used experimental modal analysis (EMA) and power spectrum density (PSD) to observe the sanding parts and the whole machine, respectively. In the modal test, we mainly adopted the cross spots testing method to get the frequency response function of the fixed spots to every excitation vibration spot, then applied the SISO frequency response function and the frequency response function fitting method to identify and complete parameter recognition, respectively. The typical frequency response function chart of the whole machine and its sanding parts, as well as its second-order mode charts of contacting roller, were obtained. Through PSD analysis, we can get the amplitude-frequency spectrum and drive frequency. Translated from Scientia Silvae Sinicae, 2005, 41(6): 132–137 [译自: 林业科学]     

Wood Moisture Content Measurement by X-Ray Exposure Method

lNTRoDUCTIONTheon-sitcnon-dcstructit'cmcasurcl11cntofu.oodmoisbocontcntattTactsgrcatintcrcsts.Itpla3'simpor-tantpartsinthescicntificrcscarchsucl1asonthchcatandmasstransportproccssesint"ooddri'ing.thcim-pregnationofliquidinxt'ood.thcmoisturccontcntdistri-b…     

Lignin Characterization of Triploid Clones of Populus tomentosa Carr.

In order to understand the structural characteristics of lignin in triploid clones ofPopulus tomentosa and its changes in the processes of pulping and bleaching, milled wood lignin （MWL）, lignin carbohydrate complex （LCC） and the residual lignin from kraft pulp （KP） and sulfite pulp （SP） were isolated and analyzed by Fourier transform infrared （FTIR） spectrum and ^13C nuclear magnetic resonance （NMR）. The most diagnostic peaks were assigned and the differences were discussed. The spectral patterns reveal that triploid P tomentosa shows the specific features of hardwood from temperate areas, but in the spectrum of FTIR, the strength ratio orAl270 cm^-1 to A1226 cm^-1 is 0.88, higher than the average of hardwood from temperate areas, which will make the lignin delignification more difficult during pulping and bleaching. The LCC from triploid P tomentosa is mainly composed of xyloglucan and glucuronic acid, and other glucides have much lower ratio. In LCC FTIR, there are three peaks at 1 427, 1 329 and 1 046 cm^-1, indicating that both semi-cellulose and cellulose could exist in LCC, and that there might be relationships between cellulose and lignin. Compared with the residual lignin from KP and SP, the condensed structure in KP is more than that in SP.     

国产人造板宽带砂光机功率谱密度和试验模态分析

以国产B229型四四砂架人造板双面宽带砂光机为研究对象,从易产生横纹缺陷入手,对其砂架部件、整机等分别采用试验模态分析(EMA)及功率谱密度法(PSD)来开展振动动态特性研究。在模态试验中,采取测量点固定、改变激振点的跑点测量方法,得到固定测量点对各激振点频响函数,并应用SISO频响函数识别法,通过频响函数曲线拟合来完成模态参数识别,获到典型的整机、砂架部件的频响函数图和接触辊的二阶振型图。通过PSD分析,获得砂光机的PSD图谱和激励频率等。     

杠杆压铊张紧系统带锯空转振动特性的分析

本文对杠杆压铊张紧系统带锯产生振动的原因,进行了试验和理论研究。用2034型频谱分析仪试验表明,带锯条振动属于复杂周期信号的离散型频谱,是由多个简谐振动叠加而成;同时理论考察分析表明,带锯条杠杆压铊张紧系统不同于秤量重物的“平衡秤”,不可能达到“静平衡”,而是在锯轮参数激振作用下形成周期性受迫振动。锯轮参数激振和杠杆压铊张紧系统位移激振之间交互作用,是使带锯条产生周期振动并引起张紧力发生变化的重要原因。     

国有林场树种结构调整及稳定性分析--以湖南省国有武冈林场为例

运用目标规划模型对湖南省国有武冈林场的森林树种结构进行优化,得到其理想的树种结构,然后计算出理想树种结构的信息熵和信息熵相对值,用于评价该场的树种结构稳定性.评价结果表明:该场1990～1999年的树种结构信息熵变化不大,稍有增势,比理想的树种结构信息熵偏小,这说明该场现有的树种结构处于过于有序状态,即,人工干扰过大,会损失某些利用功能.该评价结果可为其森林经营结构的调整提拱科学的参考依据.     

‘热引19号’坚尼草选育研究报告

1998年从澳大利亚引入坚尼草TD58(Panicum maximum‘TD58')后,相继完成适应性评价、品种比较试验、区域试验和生产试验,2007年选育而成‘热引19号'坚尼草(P.maximum'Reyin NO.19')。结果表明:该品种年均干草产量达21753.02 kg·hm~(-2),种子年均产量为800.05 kg·hm~(-2),营养价值适中,且耐低温、耐荫、耐旱、花期晚,综合性状均优于对照品种,是适合于我国南方热带亚热带地区推广种植的牧草新品种。     

基于TM数据的遥感分类方法对比研究

以香格里拉县2009年Landsat5～TM遥感影像为实验数据,利用最大似然法（MLC）以及最小距离法两种方法进行了遥感分类方法研究,主要从分类精度方面对两种方法进行了对比分析,结果表明：最大似然法分类结果明显优于最小距离法,但作为传统的分类方法,二种方法分类精度都不够高。     

AHP-熵权法结合Box Behnken响应面法优化当归微波真空干燥工艺研究

为探究当归微波真空干燥的最佳工艺参数,以甘肃定西“岷归1号”为试验材料。运用HPLC法测定不同干燥温度、切片厚度、真空度条件下当归中藁本内酯（LA）、阿魏酸（FA）、洋川芎内酯H（SH）、洋川芎内酯I（SI）、绿原酸（CA）、丁烯基苯酞（BA）、抗氧化性（DPPH）、总酚（TPC）、总黄酮（TFC）、多糖（Pc）的含量,利用AHP-熵权法计算各有效活性成分的复合权重和综合评分;以综合评分为响应值,通过Box Behnken响应面法进行优化设计,确定当归微波真空干燥的最佳工艺参数。结果表明：AHP-熵权法计算得出LA、FA、SH、SI、CA、BA、DPPH、TPC、TFC、Pc、RR的Qj值分别为0.159、0.192、0.120、0.288、0.033、0.063、0.059、0.041、0.024、0.013、0.009;Box Behnken响应面法得到的当归微波真空干燥的最优工艺条件为干燥温度50 ℃、切片厚度5 mm、真空度-0.070 MPa,此时综合评分为84.95分;此外,微观电镜结果也表明在此工艺条件下,样品质构热稳定性最好且内部出现均匀规则的蜂窝状孔隙结构。因此AHP-熵权法可用于当归微波真空干燥工艺中多目标的优化。