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1,5‐Diphenyl‐1‐pentanone (A) and 1,5‐diphenyl‐2‐penten‐1‐one (B) are natural products extracted for the first time from Stellera chamaejasme. Laboratory bioassay showed that the two products have strong contact activity and very good anti‐feedant activity against Aphis gossypii and Schizaphis graminum. Both products showed dose‐dependent relationships for both forms of activity against the two aphids, the contact activity of B being about twice that of A. Both products were inferior to methomyl in contact activity but superior in anti‐feedant activity against the two aphids. This is the first report of aphicidal activity in these two compounds, which may represent a new class of aphicide. © 2001 Society of Chemical Industry 相似文献
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Kazuo Yagi Kazuhiko Akimoto Norihiko Mimori Toshiro Miyake Masaki Kudo Kazutaka Arai Shigeru Ishii 《Pest management science》2000,56(1):65-73
A series of novel 3‐(2,4,6‐trisubstituted phenyl)uracil derivatives has been synthesised and assayed for insecticidal/acaricidal activity. The assay indicated certain requirements for optimal insecticidal activity, which can be summarised as follows: (a) the substituents on the phenyl ring should possess hydrophobicity and electron‐withdrawing properties, and the sum of their volumes determines the level of activity; (b) the substituent at the 6‐position on the uracil ring should also possess electron‐withdrawing properties and hydrophobicity, together with the correct volume; (c) the 1‐position on the uracil ring should be unsubstituted for activity against Nephotettix cincticeps and Epilachna vigintioctopunctata, but substituents with length C3 to C4 may be optimal for activity against Tetranychus urticae; (d) certain substituents at the 5‐position of the uracil ring give activity against E vigintioctopunctata and T urticae, but not against N cincticeps; (e) a thiocarbonyl group at the 2‐position of the uracil ring is less effective than a carbonyl group. Of the compounds assayed, 3‐(2,6‐dichloro‐4‐trifluoromethylphenyl)‐6‐trifluoromethyluracil showed high activity against all the species assayed. © 2000 Society of Chemical Industry 相似文献
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Cyclization of 3‐aryl‐1‐(2‐hydroxyphenyl)prop‐2‐en‐1‐ones with hydrazine hydrate in refluxing formic acid afforded the title ligands, 5‐aryl‐1‐formyl‐4,5‐dihydro‐3‐(2‐hydroxyphenyl)‐1H‐pyrazoles (HL1–HL4, Ar = Ph, 4‐CH3O‐C6H4‐, 2‐furyl, 2‐thienyl). Reaction of HL1–HL4 with the divalent metal ions, Mn2+, Co2+, Ni2+, Cu2+, and Zn2+, afforded novel complexes of the type [ML2] (M = metal ion; L = deprotonated ligand) which were characterized by elemental analyses, molecular weight determinations, molar conductances, magnetic moments and electronic and infrared spectral data. The ligands behaved as tridentate, coordinating through the phenolic oxygen after deprotonation, N‐2 of the pyrazole ring and oxygen of the 1‐formyl group. The ligands and their complexes were evaluated for growth‐inhibiting activity against four phytopathogenic fungi. Macrophomina phaseoli was generally most sensitive followed by Alternaria alternata and Colletotrichum falcatum while Fusarium oxysporum was least sensitive to the tested compounds. The ligand HL1 and its complexes showed the best activity against the fungi tested. © 2000 Society of Chemical Industry 相似文献
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The mononuclear nickel(II) complex bis(azido‐κN)bis[2,5‐bis(pyridin‐2‐yl)‐1,3,4‐thiadiazole‐κ2N2,N3]nickel(II) protects tomato from Verticillium dahliae by inhibiting fungal growth and activating plant defences 下载免费PDF全文
Hanane Zine Lalla Aicha Rifai Tayeb Koussa Fouad Bentiss Salaheddine Guesmi Abdelhakim Laachir Kacem Makroum Malika Belfaiza Mohamed Faize 《Pest management science》2017,73(1):188-197
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Phototransformation of metoxuron [3‐(3‐chloro‐4‐methoxyphenyl)‐1,1‐dimethylurea] in aqueous solution
Abdelaziz Boulkamh Dominique Harakat Tahar Sehili Pierre Boule 《Pest management science》2001,57(12):1119-1126
UV irradiation of metoxuron in aerated aqueous solution at 254 nm or between 300 and 450 nm led initially to an almost specific photohydrolysis of the C–Cl bond, resulting in the formation of 3‐(3‐hydroxy‐4‐methoxyphenyl)‐1,1‐dimethylurea (MX3) and hydrogen chloride. The quantum yield was determined to be 0.020 (±0.005) in solutions irradiated at 254 nm. Five minor photoproducts were also identified, in particular the dihydroxydimethoxybiphenyl derivatives resulting from the phototransformation of MX3. Irradiation increased the toxicity of an aqueous solution of metoxuron to the marine bacterium Vibrio fischeri. © 2001 Society of Chemical Industry 相似文献
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